Aerosol synthesis of AlN by nitridation of aluminum vapor and clusters
Identifieur interne : 001D22 ( Main/Exploration ); précédent : 001D21; suivant : 001D23Aerosol synthesis of AlN by nitridation of aluminum vapor and clusters
Auteurs : Sotiris E. Pratsinis [États-Unis] ; Guizhi Wang [États-Unis] ; Siddhartha Panda [États-Unis] ; Theresa Guiton [États-Unis] ; Alan W. Weimer [États-Unis]Source :
- Journal of Materials Research [ 0884-2914 ] ; 1995-03.
Abstract
Aluminum nitride (AlN) powders were produced in an aerosol flow reactor by direct nitridation of aluminum vapor with ammonia and nitrogen in flowing argon. In the presence of excess NH3, pure AlN powders were obtained from 1400 to 1873 K. These powders had higher specific surface areas than commercially available AlN powders. The effects of reactor temperature and gas flow rate on AlN purity, yield, and grain and crystallite size were investigated. The BET grain diameter of AlN increased as the process temperature increased, indicating sintering controlled particle formation and growth. Both the crystallite size and the BET grain size of pure AlN powders slightly decreased as ammonia flow rate was increased. Increasing temperature and flow rate increased the AlN yield.
Url:
DOI: 10.1557/JMR.1995.0512
Affiliations:
Links toward previous steps (curation, corpus...)
- to stream Istex, to step Corpus: 000F17
- to stream Istex, to step Curation: 000F17
- to stream Istex, to step Checkpoint: 000A97
- to stream Main, to step Merge: 001D96
- to stream Main, to step Curation: 001D22
Le document en format XML
<record><TEI wicri:istexFullTextTei="biblStruct"><teiHeader><fileDesc><titleStmt><title>Aerosol synthesis of AlN by nitridation of aluminum vapor and clusters</title>
<author><name sortKey="Pratsinis, Sotiris E" sort="Pratsinis, Sotiris E" uniqKey="Pratsinis S" first="Sotiris E." last="Pratsinis">Sotiris E. Pratsinis</name>
</author>
<author><name sortKey="Wang, Guizhi" sort="Wang, Guizhi" uniqKey="Wang G" first="Guizhi" last="Wang">Guizhi Wang</name>
</author>
<author><name sortKey="Panda, Siddhartha" sort="Panda, Siddhartha" uniqKey="Panda S" first="Siddhartha" last="Panda">Siddhartha Panda</name>
</author>
<author><name sortKey="Guiton, Theresa" sort="Guiton, Theresa" uniqKey="Guiton T" first="Theresa" last="Guiton">Theresa Guiton</name>
</author>
<author><name sortKey="Weimer, Alan W" sort="Weimer, Alan W" uniqKey="Weimer A" first="Alan W." last="Weimer">Alan W. Weimer</name>
</author>
</titleStmt>
<publicationStmt><idno type="wicri:source">ISTEX</idno>
<idno type="RBID">ISTEX:47E334B0270BA71277CE531E8A606E3B92235FC8</idno>
<date when="1995" year="1995">1995</date>
<idno type="doi">10.1557/JMR.1995.0512</idno>
<idno type="url">https://api.istex.fr/ark:/67375/6GQ-D1JPRTVL-H/fulltext.pdf</idno>
<idno type="wicri:Area/Istex/Corpus">000F17</idno>
<idno type="wicri:explorRef" wicri:stream="Istex" wicri:step="Corpus" wicri:corpus="ISTEX">000F17</idno>
<idno type="wicri:Area/Istex/Curation">000F17</idno>
<idno type="wicri:Area/Istex/Checkpoint">000A97</idno>
<idno type="wicri:explorRef" wicri:stream="Istex" wicri:step="Checkpoint">000A97</idno>
<idno type="wicri:doubleKey">0884-2914:1995:Pratsinis S:aerosol:synthesis:of</idno>
<idno type="wicri:Area/Main/Merge">001D96</idno>
<idno type="wicri:Area/Main/Curation">001D22</idno>
<idno type="wicri:Area/Main/Exploration">001D22</idno>
</publicationStmt>
<sourceDesc><biblStruct><analytic><title level="a">Aerosol synthesis of AlN by nitridation of aluminum vapor and clusters</title>
<author><name sortKey="Pratsinis, Sotiris E" sort="Pratsinis, Sotiris E" uniqKey="Pratsinis S" first="Sotiris E." last="Pratsinis">Sotiris E. Pratsinis</name>
<affiliation wicri:level="2"><country xml:lang="fr">États-Unis</country>
<placeName><region type="state">Ohio</region>
</placeName>
<wicri:cityArea>Department of Chemical Engineering, Center for Aerosol Processes, University of Cincinnati, Cincinnati</wicri:cityArea>
</affiliation>
</author>
<author><name sortKey="Wang, Guizhi" sort="Wang, Guizhi" uniqKey="Wang G" first="Guizhi" last="Wang">Guizhi Wang</name>
<affiliation wicri:level="2"><country xml:lang="fr">États-Unis</country>
<placeName><region type="state">Ohio</region>
</placeName>
<wicri:cityArea>Department of Chemical Engineering, Center for Aerosol Processes, University of Cincinnati, Cincinnati</wicri:cityArea>
</affiliation>
</author>
<author><name sortKey="Panda, Siddhartha" sort="Panda, Siddhartha" uniqKey="Panda S" first="Siddhartha" last="Panda">Siddhartha Panda</name>
<affiliation wicri:level="2"><country xml:lang="fr">États-Unis</country>
<placeName><region type="state">Ohio</region>
</placeName>
<wicri:cityArea>Department of Chemical Engineering, Center for Aerosol Processes, University of Cincinnati, Cincinnati</wicri:cityArea>
</affiliation>
</author>
<author><name sortKey="Guiton, Theresa" sort="Guiton, Theresa" uniqKey="Guiton T" first="Theresa" last="Guiton">Theresa Guiton</name>
<affiliation wicri:level="2"><country xml:lang="fr">États-Unis</country>
<placeName><region type="state">Michigan</region>
</placeName>
<wicri:cityArea>Advanced Ceramics Laboratory, The Dow Chemical Co., 1776 Building, Midland</wicri:cityArea>
</affiliation>
</author>
<author><name sortKey="Weimer, Alan W" sort="Weimer, Alan W" uniqKey="Weimer A" first="Alan W." last="Weimer">Alan W. Weimer</name>
<affiliation wicri:level="2"><country xml:lang="fr">États-Unis</country>
<placeName><region type="state">Michigan</region>
</placeName>
<wicri:cityArea>Advanced Ceramics Laboratory, The Dow Chemical Co., 1776 Building, Midland</wicri:cityArea>
</affiliation>
</author>
</analytic>
<monogr></monogr>
<series><title level="j">Journal of Materials Research</title>
<title level="j" type="abbrev">J. Mater. Res.</title>
<idno type="ISSN">0884-2914</idno>
<idno type="eISSN">2044-5326</idno>
<imprint><publisher>Cambridge University Press</publisher>
<pubPlace>New York, USA</pubPlace>
<date type="published" when="1995-03">1995-03</date>
<biblScope unit="volume">10</biblScope>
<biblScope unit="issue">3</biblScope>
<biblScope unit="page" from="512">512</biblScope>
<biblScope unit="page" to="520">520</biblScope>
</imprint>
<idno type="ISSN">0884-2914</idno>
</series>
</biblStruct>
</sourceDesc>
<seriesStmt><idno type="ISSN">0884-2914</idno>
</seriesStmt>
</fileDesc>
<profileDesc><textClass></textClass>
<langUsage><language ident="en">en</language>
</langUsage>
</profileDesc>
</teiHeader>
<front><div type="abstract">Aluminum nitride (AlN) powders were produced in an aerosol flow reactor by direct nitridation of aluminum vapor with ammonia and nitrogen in flowing argon. In the presence of excess NH3, pure AlN powders were obtained from 1400 to 1873 K. These powders had higher specific surface areas than commercially available AlN powders. The effects of reactor temperature and gas flow rate on AlN purity, yield, and grain and crystallite size were investigated. The BET grain diameter of AlN increased as the process temperature increased, indicating sintering controlled particle formation and growth. Both the crystallite size and the BET grain size of pure AlN powders slightly decreased as ammonia flow rate was increased. Increasing temperature and flow rate increased the AlN yield.</div>
</front>
</TEI>
<affiliations><list><country><li>États-Unis</li>
</country>
<region><li>Michigan</li>
<li>Ohio</li>
</region>
</list>
<tree><country name="États-Unis"><region name="Ohio"><name sortKey="Pratsinis, Sotiris E" sort="Pratsinis, Sotiris E" uniqKey="Pratsinis S" first="Sotiris E." last="Pratsinis">Sotiris E. Pratsinis</name>
</region>
<name sortKey="Guiton, Theresa" sort="Guiton, Theresa" uniqKey="Guiton T" first="Theresa" last="Guiton">Theresa Guiton</name>
<name sortKey="Panda, Siddhartha" sort="Panda, Siddhartha" uniqKey="Panda S" first="Siddhartha" last="Panda">Siddhartha Panda</name>
<name sortKey="Wang, Guizhi" sort="Wang, Guizhi" uniqKey="Wang G" first="Guizhi" last="Wang">Guizhi Wang</name>
<name sortKey="Weimer, Alan W" sort="Weimer, Alan W" uniqKey="Weimer A" first="Alan W." last="Weimer">Alan W. Weimer</name>
</country>
</tree>
</affiliations>
</record>
Pour manipuler ce document sous Unix (Dilib)
EXPLOR_STEP=$WICRI_ROOT/Sante/explor/H2N2V1/Data/Main/Exploration
HfdSelect -h $EXPLOR_STEP/biblio.hfd -nk 001D22 | SxmlIndent | more
Ou
HfdSelect -h $EXPLOR_AREA/Data/Main/Exploration/biblio.hfd -nk 001D22 | SxmlIndent | more
Pour mettre un lien sur cette page dans le réseau Wicri
{{Explor lien |wiki= Sante |area= H2N2V1 |flux= Main |étape= Exploration |type= RBID |clé= ISTEX:47E334B0270BA71277CE531E8A606E3B92235FC8 |texte= Aerosol synthesis of AlN by nitridation of aluminum vapor and clusters }}
This area was generated with Dilib version V0.6.33. |